WS 2013 SS 2013
WS 2012
WS 2011 SS 2012
Department of Chemistry
open physics
KVL / Klausuren / MAP 1st HS: 15.10  2nd HS: 10.12  sem.br.: 16.02  begin SS: 06.04

2020125194 NMR spectroscopy (1st HS)  VVZ 

VL
Mon 9-11
weekly NEW 14 0'07 (120) Clemens Mügge
Tue 15-17
weekly NEW 14 0'07 (120)
Aims
1.Basic understandig of NMR experiment:
Principle of method, instrumentation, NMR spectrum.

2.Spectrum analysis and interpretation:
Identification of spectral data and transformation in structure information (constitution, configuration,conformation).

3.Modern NMR techniques: 1D,2D,nD.

4.Knowledge of applications of NMR
Requirements
successful conclusion of modul AU2
Structure / topics / contents
1.Physical basics:
Nuclear magetism,nuclear magnetic resonance, relaxation.
2.Instrumentation:
Equipment configuration, PFT technique, magnet system, transmitter, receiver, quality criteria.
3.NMR spectrum, spectral parameters:
Chemical shifts, coupling constants,signal intensity, T1, T2, NOE's.
4.Spectrum analysis and interpretation:
1H,13C,19F,31P spectra, analysis algorithm.
5.1D,2D,nD NMR techniques:
COSY,TOCSY,NOESY,EXSY,HMQC,HMBC,1D-COSY,...
6.Applications:
Org. and inorg.chemistry, bio-,enviromental and food chemistry, medicine.
Assigned modules
AU3
Amount, credit points; Exam / major course assessment
2 SWS, 0 SP/ECTS (Arbeitsanteil im Modul für diese Lehrveranstaltung, nicht verbindlich)
Teil-Klausur (60min.)
über den Stoff der NMR-Vorlesung und -Übung
Contact
Clemens Mügge, R 0 103
Literature
Günther,Harald. NMR-Spektroskopie. Georg Thieme Verlag
Friebolin,Horst. 1D- und 2D-NMR-Spektroskopie . VCH
Hesse,M.,Meier,H.,Zeeh,B.. Spektroskopische Methoden in der Organischen Chemie. Georg Thieme Verlag
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