WS 2014 SS 2014
WS 2013
WS 2012 SS 2013
Department of Chemistry
open physics
KVL / Klausuren / MAP 1st HS: 14.10  2nd HS: 09.12  sem.br.: 17.02  begin SS: 12.04

2020135018 NMR spectroscopy (1st HS)  VVZ 

VL
Mon 9-11
weekly NEW 14 0'07 (120) Clemens Mügge
Tue 15-17
weekly NEW 14 0'07 (120)
Aims
1.Basic understandig of NMR experiment:
Principle of method, instrumentation, NMR spectrum.

2.Spectrum analysis and interpretation:
Identification of spectral data and transformation in structure information (constitution, configuration,conformation).

3.Modern NMR techniques: 1D,2D,nD.

4.Knowledge of applications of NMR
Requirements
successful conclusion of modul AU2
Structure / topics / contents
1.Physical basics:
Nuclear magnetism,nuclear magnetic resonance, relaxation.
2.Instrumentation:
Equipment configuration, PFT technique, magnet system, transmitter, receiver, quality criteria.
3.NMR spectrum and spectral parameters:
chemical shifts, coupling constants,signal intensity,LB,T1,NOE's.
4.Spectrum analysis and interpretation:
1H,13C,19F,31P spectra,spectrum analysis algorithm.
5.1D,2D,nD NMR techniques:
COSY,TOCSY,NOESY,EXSY,HMQC,HMBC,1D-COSY,...
6.Applications:
Org. and inorg.chemistry, bio-,enviromental and food chemistry, medicine
Assigned modules
AU3
Amount, credit points; Exam / major course assessment
2 SWS, 2 SP/ECTS (Arbeitsanteil im Modul für diese Lehrveranstaltung, nicht verbindlich)
Written examination, part I (60 min.)
about NMR lectures und exercises
Contact
Clemens Mügge, IfC, Brook-Taylor-Str.2, R 0 103
Literature
Günther,Harald. NMR-Spektroskopie. Georg Thieme Verlag
Friebolin,Horst. 1D- und 2D-NMR-Spektroskopie . VCH
Hesse,M.,Meier,H.,Zeeh,B.. Spektroskopische Methoden in der Organischen Chemie. Georg Thieme Verlag
Berger,S.. 200 and more NMR experiments. Wiley-VCH
Levitt,M.H.. Spin dynamics. John Wiley and Sons
Keeler,J.. Understanding NMR spectroscopy. John Wiley and Sons
Meusinger,R.. NMR-Spektren richtig ausgewertet. Springer
Breitmeier,E.. Vom NMR-Spektrum zur Strukturformel organischer Verbindungen. Wiley-VCH
Mitechell,T.N.,Costicella,B.. NMR- from spectra to structures. Springer
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