2020145119 NMR spectroscopy
(1st HS)
Digital- & Präsenz-basierter Kurs
- classroom language
- DE
- aims
- 1.Basic understandig of NMR experiment:
Principle of method, instrumentation, NMR spectrum.
2.Spectrum analysis and interpretation:
Identification of spectral data and transformation in structure information (constitution, configuration,conformation).
3.Modern NMR techniques: 1D,2D,nD.
4.Knowledge of applications of NMR
- requirements
- successful conclusion of modul AU2
- structure / topics / contents
- 1.Physical basics:
Nuclear magnetism,nuclear magnetic resonance, relaxation.
2.Instrumentation:
PFT technique,Equipment configuration,magnet system, transmitter, receiver, quality criteria.
3.NMR spectrum and spectral parameters:
chemical shifts, coupling constants,signal intensity,LB,T1,NOE's.
4.Spectrum analysis and interpretation:
1H,13C,19F,31P spectra,spectrum analysis algorithm.
5.1D,2D,nD NMR techniques:
COSY,TOCSY,NOESY,EXSY,HMQC,HMBC,1D-COSY,...
6.Applications:
Org. and inorg.chemistry, bio-,enviromental and food chemistry, medicine
- assigned modules
-
AU3
- amount, credit points; Exam / major course assessment
- 2 SWS, 2 SP/ECTS (Arbeitsanteil im Modul für diese Lehrveranstaltung, nicht verbindlich)
Written examination, part I (60 min.)
about NMR lectures und exercises
- contact
- Prof. Clemens Mügge, IfC, Brook-Taylor-Str.2, R 0 103
- literature
-
Günther,Harald. NMR-Spektroskopie. Georg Thieme Verlag
Friebolin,Horst. 1D- und 2D-NMR-Spektroskopie . VCH
Hesse,M.,Meier,H.,Zeeh,B.. Spektroskopische Methoden in der Organischen Chemie. Georg Thieme Verlag
Berger,S.. 200 and more NMR experiments. Wiley-VCH
Levitt,M.H.. Spin dynamics. John Wiley and Sons
Keeler,J.. Understanding NMR spectroscopy. John Wiley and Sons
Meusinger,R.. NMR-Spektren richtig ausgewertet. Springer
Breitmeier,E.. Vom NMR-Spektrum zur Strukturformel organischer Verbindungen. Wiley-VCH
Mitechell,T.N.,Costicella,B.. NMR- from spectra to structures. Springer